李 政¹，何 浩^1*，朱 礼²，方 群¹

（1.湖南省产商品质量检验研究院，长沙410007；2.岳阳市检验检测中心，岳阳414000）

摘要：该文通过气相色谱法检测6种醇类物质。样品经丙酮振荡提取，气相色谱-外标法定量，6种目标物质在40 min内实现分离，分离度均大于1.5，线性范围为5～500 μg/mL，相关系数（r2）为0.999 0～0.999 9，方法检出限为0.001～0.002 g/kg，方法定量限为0.003～0.006 g/kg，加标回收率为98.0%～109.8%，相对标准偏差（RSD）为1.48%～7.43%。

关键词：气相色谱法；醇类物质；检测

中图分类号：TS207.3 文献标识码：A 文章编号：1674-506X（2024）06-0142-0003

Establishment of a Gas Chromatography Method for Detecting Six Types of Alcohol Substances

LI Zheng¹，HE Hao^1*，ZHU Li²，FANG Qun¹

（1.Hunan Provincial Institute of Commodity Quality Inspection，Changsha 410007，China；2.Yueyang Inspection and Testing Center，Yueyang 414000，China）

Abstract：In this paper, gas chromatography was used to detect six types of alcohol substances. The sample was extracted by acetone oscillation and quantified by gas chromatography external standard method. Six target substances were separated within 40min,with all resolutions greater than 1.5 and a linear range of 5～500μg/mL, with a correlation coefficient r2 of 0.999 0～0.999 9. The detection limit of the method was 0.001～0.002 g/kg, the quantitative limit of the method was 0.003～0.006 g/kg, the spiked recovery rate was 98.0%～109.8%,and the relative standard deviation (RSD) was 1.48%～7.43%.

Keywords：gas chromatography；alcohol substance；detection

doi：10.3969/j.issn.1674-506X.2024.06-022